Ewch i’r prif gynnwys

Analytical SEM (Scanning Electron Microscope)

Our state-of-the-art Zeiss Sigma HD Field Emission Gun Analytical SEM (ASEM) is the flagship of our facility.

Brand/model Zeiss NTS S360 SEM with Oxford Instruments INCA Energy Plus
Manylion Conventional W filament, high vacuum, scanning electron microscope, calibrated with full set of element standards for analysis of polished material surfaces. Fitted with secondary and backscattered electron detectors and EDX and WDX spectrometers.
Cyfleuster Electron microbeam facility
Ysgol Ysgol Gwyddorau'r Ddaear a'r Amgylchedd

The ASEM is equipped with:

  • an in-lens and Everhart-Thornley secondary electron detector
  • a backscatter electron detector
  • two Oxford Instruments 150 mm2 energy dispersive X-ray spectrometers (EDS)
  • an Oxford Instruments Wave wavelength dispersive X-ray spectrometer (WDS)
  • an iXRF micro-XRF source
  • an Oxford Instruments Aztec electron back-scatter diffraction (EBSD) detector
  • a Centaurus cathodoluminescence detector

A combination of EDS (for major and minor elements), WDS (for high-precision analysis of major and minor elements) and micro-XRF (for trace elements) means complete characterization of elements heavier than carbon can be achieved with accuracy and precision rivalling an electron microprobe.

The dual 150 mm2 EDS detectors, which can capture in excess of 1 000 000 counts per second, enable rapid, high-resolution 2D mapping of distributions of major and minor elements over relatively large areas. Since the ASEM is fully standardized, the element maps are quantitative, thus absolute element abundances can be mapped. In addition, using the micro-XRF source with an accelerating voltage of 50 kV, trace element distributions of elements heavier than Ti22 can be imaged with a resolution of 15 µm.

EBSD provides information on crystal orientations with sub-micron resolution and can be combined with EDS chemical data for textural and microstructural studies. Image referencing software allows easy navigation around the sample using images from a flatbed scanner or digital camera.

Cysylltwch

Dr Duncan Muir

Email
muird1@cardiff.ac.uk
Telephone
+44 (0)29 2087 5059

Lleoliad

Main Building
Plas y Parc
CF10 3AT